Technologie Hero Istock-695675608 Jaczhou

Methods

I’m a materials scientist — so why should I care about neutrons?

Short answer:
Neutrons allow us to non-destructively investigate the structure and dynamics of matter across a wide range of length scales — from atomic (1 Å) to macroscopic (millimeters)!

Longer answer:
Despite being challenging (and costly) to produce, neutrons offer unique advantages that make them an invaluable probe in materials science and many other fields:

  • Ideal wavelength: Neutrons have wavelengths comparable to interatomic distances, making them perfect for studying molecular structures. The interference patterns from scattered neutrons reveal the spatial arrangement of atoms and molecules in a sample.
  • Electrically neutral: Because neutrons carry no charge, they interact only weakly with matter. This minimizes beam-induced damage and allows for the investigation of thick or dense samples that would be inaccessible with other techniques.
  • Magnetic sensitivity: Neutrons behave like tiny magnets, enabling the study of magnetic field distributions and magnetic properties of materials. For example, different phases in metallic alloys often exhibit distinct magnetic behaviors — a key insight for materials development.
  • Isotope sensitivity: Chemically, isotopes of an element behave similarly. However, neutrons interact differently with each isotope. This property is exploited by selectively substituting atoms to act as "markers", allowing detailed studies of:
    ◦ Crystallographic structures
    ◦ Hydrogen storage materials
    ◦ Biological systems
    ◦ Lithium distribution in electrochemical devices
Neutron imaging
Neutron reflectometry
Small angle neutron scattering
Texture analysis and Stress-/Strain measurement
Environmental Scanning Electron Microscopy
Dilatometry
3D-scanning and printing

The following instruments are available:

STRESS-SPEC

STRESS-SPEC: View of instrument

[ Photo: Astrid Eckert / TUM]

for stress, texture, or phase analysis

E-mail

Contact: Dr. Weimin Gan


SANS-1

Sans-1: Look into the detector tube

[Photo: Sebastian Mast]

for studies of the nanostructure of bulk samples

E-mail

Contact: Dr. André Heinemann


REFSANS

Refsans instrument

[Photo: Wenzel Schürmann / TUM]

for studies of nanostructures at interfaces

E-mail

Contact: Dr. Jean-François Moulin


Materials Science Lab

for sample preparation and complementary characterisation

E-mail

Contact: Armin Kriele


The most important methods:

• Diffraction – strain analysis

For measurements of stresses in the interior of materials and components.

• Diffraction – texture measurements

For measurements of crystallographic textures.

• Diffraction – phase analysis

For the quantitative determination of the phase composition of a material.

• Small-Angle Neutron Scattering (SANS)

For the analysis of nanostructures in the bulk, e.g. precipitates.

• Neutronen-reflectometry and small-angle scattering under grazing incidence (GISANS)

For the analysis of nanostructuires at interfaces, e.g. coatings.